Synthesis of Carbon Nanomaterials Using Stainless Steel Type 304 as Substrate and Catalyst by Chemical Vapor Deposition Method
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Abstract
This research aim is to study the direct synthesis of carbon nanomaterials by chemical vapor deposition using 304 stainless steel as both catalyst and substrate at 650°C. The ratio of mixing gases (acetylene, hydrogen and nitrogen) in chamber is controlled to constant value at 1:1:2 with a total flow rate of 400 ml/min for 20 min. Besides that, the surface treatment of 304 stainless steel substrate was performed in the atmospheric of hydrogen and nitrogen before providing acetylene as a carbon source for 15 min. The microphotograph results from FE-SEM and TEM can be used in order to investigate the physical morphology of the obtained carbon nanomaterials. Three types of carbon nanomaterials that can be synthesized are carbon nanotubes, carbon fibers and bamboo carbon nanotubes.
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Engineering Research Articles
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References
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[10] M. Hashempour, A. Vicenzo, F. Zhao, and M. Bestetti, “Direct growth of MWCNTs on 316 stainless steel by chemical vapor deposition: Effect of surface nano-features on CNT growth and structure,” Carbon, vol. 63, pp. 330–347, 2013.
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[13] L. Camilli, P. Castrucci, M. Scarselli, E. Gautron, S. Lefrant, and MD. Crescenzi, “Probing the structure of Fe nanoparticles in multiwall carbon nanotubes grown on a stainless steel substrate,” Journal of Nanoparticle Research, vol.15, pp.1–9, 2013.
[14] D. A. Jones, Principles and prevention of corrosion. Macmillan Publishing Company, pp. 151–158, 1996.
[15] S. Kruehong, C. Kruehong, and A. Artnaseaw, “Branched carbon fibres and other carbon nanomaterials grown directly from 304 stainless steel using a chemical vapour deposition process,” Diamond and Related Materials, vol. 64, pp. 143–152, 2016.
[16] C. Masarapu and B. Wei, “Direct growth of aligned multiwalled carbon nanotubes on treated stainless steel substrates,” Langmuir, vol. 23, no. 17, pp. 9046–9049, 2007.
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[18] V. Asokan, D. N. Madsen, P. Kosinski, and V. Myrseth, “Transformation of carbon black into carbon nano-beads and nanotubes: The effect of catalysts,” New Carbon Materials, vol. 30, pp. 904–910, 2015.
