Design of experiments to analyze factors for block digestion affecting the defect of nitrogen tubes

10.14416/j.ind.tech.2025.08.011

Authors

  • Yossawat Cheewaworanontree Program in Industrial Management, Engineering and Industrial Technology, Bansomdejchaopraya Rajabhat University
  • Kridtharit Thongsin Program in Industrial Engineering and Supply Chain Management, Engineering and Industrial Technology, Bansomdejchaopraya Rajabhat University
  • Piya Rontlaong Program in Industrial Engineering and Supply Chain Management, Engineering and Industrial Technology, Bansomdejchaopraya Rajabhat University

Keywords:

Factorial design, reducing defect, digestion tube

Abstract

This research aims to reduce the waste of nitrogen tubes generated from testing for the quantities of Nitrogen and crude protein in laboratory settings of a case study factory, using 2k Full Factorial Design. The study to identify factors and their levels in adjusting the settings of the Block Digestion machine appropriately. The experimental design comprises three main factors: temperature, burning time, and cooling time. The experiments were repeated three times, totaling 24 trials. The experimental results indicated that temperature, burning time, and cooling time had a statistically significant effect on the occurrence of cracks in the test tubes at the 95% confidence level. Moreover, significant interaction effects were observed between temperature and burning time, as well as between temperature and cooling time and the appropriate factors and levels for adjusting the settings of the Block Digestion machine are: temperature at 400 degrees celsius, burning time of 120 minutes, and cooling time of 50 minutes. Subsequently, the appropriate factors and levels were used to collect data for comparison before and after adjustment. It was found that before adjustment, there were 359 instances of tube damage, whereas after adjustment, the instances reduced to 7, resulting in a reduction of waste by 98.05%. When comparing the expenses incurred, it was found that before adjustment, the cost of the 359 damaged tubes amounted to 502,600 baht, with a unit cost of 1,400 baht per tube. After adjustment, with only 7 damaged tubes, the cost amounted to 9,800 baht, resulting in a reduction in expenses by 492,800 baht.

References

Y. Cheewaworanontree, P. Rontlaong, K. Thongsin and T. Teekasap, Reducing waste in the clutch assembly pumping process case study: Automotive air compressor factory, The Journal of Industrial Technology, Suan Sunandha Rajabhat University, 2023, 11(2), 27-38. (in Thai)

T. Thepchu, S. Rakkran, P. Sriwichian and J. Plongmai, Defect reduction in process for shampoo a design of engineering, Journal of Science and Technology, Sukhothai Thammathirat Open University, 2022, 2(1), 47-55. (in Thai)

T. Sunarak, Defect reduction in the welding process of motocycle STAY R-L Parts, The Journal of Industrial Technology, Suan Sunandha Rajabhat University, 2018, 6(1), 6-15. (in Thai)

S. Suwanauksorn and C. Pornsing, A Study of factors for chemical cost reduction in the brake pad manufacturing process, The Journal of Industrial Technology, 2021,17(1), 31-52. (in Thai)

Y. Jantana and N. Rattanawai, Optimizing factors for lemongrass slicer using design of experiment, Science and Technology Nakhon Sawan Rajabhat University Journal, 2022, 14(19), 83-95. (in Thai)

K. Noirach and P. Chutima, Defective reduction from welding splash in motorcycle battery production process, Research and Development Journal, 2014, 25(3), 55-61. (in Thai)

P. Siri-O-Ran and J. Pummak, Weight loss reduction in pineapple pie production process, Thai Industrial Engineering Network Journal, 2022, 6(1), 48-53. (in Thai)

D.C. Montgomery, Introduction to statistical quality control, 4th Edition, John Wiley and Sons, Inc., NJ, USA, 2002.

B. Sao-siw and N. Sokul, Reducing defects in packaging by applying experimental results: A case study of a snack company, Industrial Technology Lampang Rajabhat University Journal, 2016, 9(2), 30-44. (in Thai)

H. Su, H.M. Yao, H. Zeng, The optimization research of the multi-response problems based on the SUR. Pakistan Journal of Pharmaceutical Sciences, 2015, 28(2 Supplement), 731-737.

A. Leenatham and P. Khemavuk, Process improvement of PTCA guide wire by using design of experiment, Srinakharinwirot University Engineering Journal, 2019, 14(2), 12-24. (in Thai)

P. Parakawong Na Ayuthaya, A design of experiment to waste reduction injection process of electronic parts, Thesis, Silpakorn University, Thailand, 2018. (in Thai)

Downloads

Published

2025-08-20

Issue

Section

บทความวิจัย (Research article)